Ture was stirredas described above. Yield was mgchange and solutionblue mixture.
Ture was stirredas described above. Yield was mgchange and solutionblue mixture. The mL, was purified for 24 h, causing polymer 183 precipitated inand collected by filtration. The1.0 mmol)was resuspendedthechlorobenzene (25 mL), of a dark to violet. The polymer polymer was added, and in a Benidipine manufacturer gradual colour (73 ) anhydrousto violet powder.mL, 1.0 mmol) was as described above. Yield 183 mg (73 )of your collected by filtration. The product as a dark violet. The polymer was was resuspended in chlorobenzenecolor adjust and option hydrazine (0.03 polymer purified added, causing a gradual (25 mL), as well as the solution to violet. powder. item as hydrazine (0.03 polymer was was added, causing gradual colour modify of anhydrous a dark violetThemL, 1.0 mmol)purified as describedaabove. Yield 183 mg (73 ) Table 3. Weight-average molecular answer to)dark violet powder. was purified of polymerization (Xw ) Yield 183 mg (73 ) item as a in g/mol and weight-average degree as described above. for polymers the weight (Mw violet. The polymer Table three. by FeCl3 -initiated oxidative polymerization beneath diverse situations. Mw of polymerization (Xw) in the synthesized Weight-average molecular weight (Mw) in g/mol and weight-average degreevalues have been determinedfor polymers product as a dark violet powder.Addition FeCl3 Time (g/mol) Yield Xw Addition FeCl Time (g/mol) 20 20 Methyl jasmonate Formula Reverse Equivalents 2.3 24 24 h h 73 73 6300 w Reverse two.three 3 6300 M Order of Reaction Yield 73 Xw20 Entry Structure Acronym Reverse two.3 24 6300 21 Reverse 1 two.3 24 h 80 5200 three 17 FeCl3 Timeh (g/mol) PEDOT-C12 Addition 1 three 2 2.3 24 h 80 Reverse 5200 Reverse two.three 5200 1720 17 three Common 1 two.3 24 h h 26 20,000 3 65 12 Reverse 2.3 2424 h 7380 6300 PEDOT-C12 1 three Regular two.three 24 h 26 20,000 three 6517 20,000 65 two.3 5200 32 Normal 2.three 2424 h h 26 80 PEDOT-C12 Reverse four Normal four 24 h 58 231,000 747 three Normal two.3 24 h 26 20,000 65 PEDOT-C12 four four Normal 231,000 747 747 Standard 44 24 h 24 h 58 58 231,000 Reverse two.3 24 h 42 5200 3 18 five 4 Common 4 24 h 58 231,000 747 Reverse 2.three 24 24 h h h 24 42 78 42 5200 three three three 18 18 two Reverse two.3 5200 five 56 Standard 2.3 5200 18 PBHOT Normal 78 5200 18 7 Normal 42.three 24 h 11 2 5200 3 3 three 18 99 28,000 Normal 2.3 242424 h h h 78 two 42 PBHOT Reverse 2.3 5200 18 56 6 PBHOT Standard 24 11 28,000 99 87 Common 44 48 h h h 102 28,000 three 9918 90,000 318 six Typical 2.three 5200 Common four 2424 h 11 78 7 PBHOT 8 Normal four 48 h ten 90,000 318 9 Reverse two.3 24 h 75 150,000 904 7 Typical 4 24 h 11 28,000 99 Common 4 48 h 10 90,000 318 8109 Reverse two.three 24 75 150,000 318 904 Regular two.three 24 h h h 26 81,000 488 8 Regular four 48 10 90,000 P3HT ten Normal 2.3 24 h 26 150,000 81,000 904395 488 Normal four 24 h 25 65,000 Reverse two.three 2424 h h 75 75 9 Reverse two.three 150,000 904 911 P3HT Regular 65,000 395 12 Common four 48 h h 72 65,000 1011 Typical 2.34 2424 h 2625 81,000 81,000 488395 488 Standard two.3 24 h 26 10 P3HT P3HT 1 12Chloroform was employed as a solvent rather of chlorobenzene. 2 Unique work-up procedure (see experimental section). 3395 Normal 4 48 h 72 65,000 11 Normal four 24 h 25 65,000 395 Entry Structure AcronymStandard four 24 h 25 65,000 395 11 Beneath the reduce limit of the a solvent rather of chlorobenzene. two Unique work-up procedure (see experimental section). 3 1 Chloroform was utilized as calibrated region from the analytical column. 12 Regular four 48 h 72 65,000 395 Typical 4 48 h 72 65,000 395 12 1 Beneath the decrease limit of your calibrated region from the analytical co.